This month I studied the books which I bought to the projekt:
1) Bulk Nanostructured Materials; Michael J. Zehetbauer, Yuntian Theodore Zhu, John Wiley & Sons, 2009;
2) Introduction to Texture Analysis: Macrotexture, Microtexture, and Orientation Mapping; Olaf Engler, Valerie Randle, CRC Press, wyd. 2, 2009.

In September I participated in session B courses organized as a part of European School on Nanosciences and Nanotechnologies (ESONN'2012) in Grenoble - France. That was the ninth edition of three-week summer school aimed at providing training for PhD students in the field of nanotechnologies and nanosciences. The academic and practical courses covered aspects such as the elaboration, characterization and functionalities of objects in “nano” scale. The program was directed to highlight the fundamental and technological advances in Nanoelectronics (session A) and at the interface between Physics, Chemistry and Biology (Session B). This two sessions were run in parallel but all participants shared common lectures and practicals.

Lectures for session B (18 x 1h45):
- Advanced biophysics to study molecular systems – given by R. Hovius, J. Piguet, Lausanne, Switzerland
- Microfluidics for Lab-on-chips – given by J.B. Salmon, Bordeaux, France
- Nano-objects synthesis – given by M. Brust, Liverpool, UK
- Surface and molecular physico-chemistry – given by R. Richter, San Sebastian, Spain
- Mechanics of molecules and biological structures – given by B. Hoogenboom, London, UK
- Drug delivery by nanoparticles – given by B. Pitard, Angers and C. Passirani, Nantes, France

Common lectures (9 x 1h45):
- Near-field microscopies – given by H. Hug, Basel, Switzerland
- Self-assembled systems and materials – given by M. Boncheva, Geneve, Switzerland
- Technology of nanofabrication – given by G. Faini, Marcoussis, France
- From research to business with nanotechnologies – given by V. Mangematin, Grenoble, France

Practicals:
- “BioChips” Introduction to DNA microarray technology and application to comparative genomic hybridization
- Droplets for the study of membrane protein
- Atomic Force Microscopy
- Study of biomolecular interactions by surface Plasmon resonance biosensor analysis (BIAcore technology)\
- Initiation to Confocal Laser Scanning Microscopy: An application to study the colocalization of adhesion cell proteins

Seminars:
- STMicroelectronics – given by D. Thomas
- Cytoo cell architects: scientific and commercial story – given by F. Chatelain, Cytoo
- An introduction to ethics: What role for ethical questioning in a scientific’s life? – given by N. Farouki, CEA Grenoble

In September we decided that KoBo extrusion / deformation experiments with high purity Zinc need to be repeated. Some of the previous samples have been analyzed after significant amount of time from original extrusion process. Some others were analyzed after much shorter time. Discrepancies in mean grain sizes observed in those two cases (much smaller grain in 'younger' sample), points to possibility of some recrystallization processes that might occur even in room temperature.
Therefore new samples of zinc after KoBo from now on are kept in liquid nitrogen in order to prevent uncontrolled recrystallization. New samples similarly to the old ones have been extruded from 40 mm diameter ingot to 1,8 mm wire in room temperature. During extrusion process, wire have been cooled with water, and immediately after extrusion samples have been cut and placed in dewar with liquid nitrogen.

The plan set in September was carrier lifetime measurements for silicon after acid texturization. The results were inconsistent with the expected (derived from the literature) because of occurring in wafers surface recombination prevented accurate measurement. For the correct measurement it is required to passivate the surface of silicon wafer what is planned for October.

In September I’ve continued the the voltammetric studies on a copper surfaces, from stable homogeneous Zn(II)-Mo(VI) citrate baths with various concetrations of sodium citrate and sodium molybdate. The voltammetric measurements were performer in a tree-electrode cell , by means of potentiostat PARSTAT 2273 or PGSTAT302N. A copper disc was the working electrode (surface area 2.83 cm2). A platinum sheet (5cm2) was used as the counter electrode. The working electrode potentials were referred to the saturated calomel electrode (SCE) and were ohmic drop, as measured by the current interrupt method, was compensated for.